Contemporary pharmaceutical and cosmetic products, particularly dispersed systems, necessitate precise control over their physicochemical characteristics. Particle size is a critical factor that substantially affects the bioavailability, stability, and overall efficacy of formulations. In this study, the “Emulzamaj” cosmetic preparation (composition 1) was analyzed using the Nanosizer NS300 (Malvern) to determine the size distribution of dispersed phases, polydispersity index (PDI), diffusion coefficient, and colloidal stability. The dispersed phase particles exhibited an average diameter of 1,149.64 nm, a PDI of 0.378, and a diffusion coefficient of 2.13 × 10⁻⁹ cm²/s. The measured zeta potential of 37.70 mV indicates good electrokinetic stability, suggesting the formulation is suitable for prolonged shelf-life and enhanced performance in cosmetic applications. These findings provide valuable insights into the formulation design and quality control of complex emulsion-based cosmetic systems.